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Handbook of synthetic organic chemistry / Michael C. Pirrung.

By: Pirrung, Michael.
Material type: materialTypeLabelBookPublisher: London : Academic Press, / Elsevier, c.2017Edition: 2nd ed.Description: xii, 272 p. : ill. (some col.) ; 24 cm.ISBN: 9780128095812.Other title: Synthetic organic chemistry.Subject(s): Organic compounds -- Synthesis | | Engineering, Chemical March2019DDC classification: 547
Contents:
1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints
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Item type Current location Collection Call number Vol info Status Date due Barcode Item holds
Book - Borrowing Book - Borrowing Central Library
First floor
Baccah 547 PIR (Browse shelf) 173 Available 000043262
Total holds: 0

Includes bibliographical references and index.

1. Safety
2. Searching the literature
3. Reagents
4. Gases
5. Reactions on a small scale -- 1-25 mmol
6. Temperature control
7. Solvents
8. The research notebook
9. Conducting the reaction itself
10. Following the reaction
11. Working up reactions
12. Evaporation
13. Vacuum systems
14. Purification of products
15. Methods for structure elucidation
16. Cleaning up after the reaction
17. Specific examples
18. Strategies for reaction optimization
Appendices
1. Safety protocols
2. Synthetic solvent selection chart
3. Solvent miscibility
4. Freezing points of common organic solvents
5. Toxicities of common organic solvents
6. Recipes for TLC stains
7. NMR spectral data of common contaminants of organic and organometallic reaction products
8. Acidities of organic functional groups
9. Acidities of organic functional groups in DMSO
10. Stuck joints

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